Sulfuric Acid
Sulfuric acid is undoubtedly the most important raw material in the chemical and pharmaceutical industry today. This fact is not unique to the United States, but is true on a worldwide basis. One can often look to the production and/or use of sulfuric acid as an indication of the industrial activity of a nation. Few chemicals are manufactured without sulfuric acid being involved. It is a strong dibasic acid and can be a reducing acid, an oxidizing acid, and/or a dehydrating agent. In the chemical industry, sulfuric acid has many diverse applications. The largest quantities are used to manufacture phosphate and nitrogen based fertilizers. The petrochemical sector utilizes sulfuric acid in alkylation and paraffin refining. The inorganic branch of the chemical industry uses sulfuric acid in the production of chromic and hydrofluoric acids, aluminum sulfate and sodium sulfate. The organic arm employs sulfuric acid in the manufacture of explosives, soaps, detergents, dyes, isocyanates, plastics, pharmaceuticals, etc. Everywhere one turns today, we encounter products which use sulfuric acid in their manufacturing process. Many chemical plants use sulfuric acid in one or more process steps and this generally results in severe corrosion problems. Each process has unique minor constituents that can change the way metals corrode. Zirconium has been used very successfully in many sulfuric acid applications. The advantage of zirconium is that corrosion rate will be very small if properly applied and equipment life of over 20 years is expected. Since there is no corrosion maintenance, repair, downtime and replacement costs do not exist and will quickly pay back for the slightly higher initial cost.
Corrosion Resistance of Zirconium and Other Metals in H2SO4
Concentration (%) Temp. (ºC) Zr 702 310L S.S. 316L S.S. Alloy B-2 Alloy C-276
10 102* < 0.1 45 574 < 1 7.0
30 108* < 0.1 1,137 5,000 2 55
55 132* 0.1 350,000 10,000 1.89 295
55 168 19.6 - - 37 212
2 225 < 0.1 - - 14.9 39.7
5 232 0.1 - - 110 153
10 225 0.1 - - 1,023 661
* boiling point
Acetic Acid
Acetic acid is one of the basic components in a wide range of organic materials including acetate esters, acetic anhydride, terephthalic acid, aspirin and other pharmaceuticals. Zirconium is considered the most corrosion resistant material in virtually all acetic acid solutions. The few exceptions include acetic acid containing cupric ions, free chlorine and solutions with insufficient moisture to allow zirconium to reform its protective oxide surface layer. Under highly stressed conditions, >650-ppm water is required in acetic acid to prevent stress corrosion cracking. If water addition is not practical, stress relieving may be considered.

View table of of Zirconium Corrosion in various acetic acid solutions

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